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Description

In general, the process would take 12 to 15 minutes

0.33g of the crude Boc-His (Trt) -Aib-OSu and 1g of the compound 2 obtained in example 3 were dissolved in 20mL of N, N-dimethylformamide, 2mL of N, N-diisopropylethylamine was added, and the reaction was carried out at room temperature for 8 hours to obtain compound 4 with a purity of 74.08%, and a specific liquid phase diagram is shown in FIG