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the folate-containing peptidyl fragment Pte-Glu-(AA) n -NH(CHR 2 )C0 2 H (3) is prepared by a polymer-supported sequential approach using standard methods, such as the Fmoc-strategy on an acid- sensitive Fmoc-AA-Wang resin (1), as shown in the following Scheme: Scheme R is Fmoc R 2 is the desired appropriately-protected amino acid side chain DIPEA is TBAF tetrabutylammonium fluoride Appropriately protected amino acid building blocks such as Fmoc-Glu-OiBu, Fmoc-D-Glu-OiBu dressing N 10 -TFA-Pte-OH, and the like, are used, as described in the Scheme, and represented in step (b) by Fmoc-AA-OH

Thermospray liquid chromatography/mass spectrometry for the analysis of L-carnitine and its short-chain acyl derivatives

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This study will tell us whether taking an l-carnitine supplement along with a pomegranate extract may be better than taking the supplement on its own.

M., Maccio, A., and Mantovani, G