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The initial twice-daily formulation was discontinued due to exceptionally high rates of gastrointestinal adverse events (nausea and vomiting), leading to discontinuation rates exceeding 50% in trials

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2.9.4 Lipid peroxidation (MDA) Lipid peroxidation was quantified by measuring malondialdehyde (MDA) levels using the thiobarbituric acid reactive substances (TBARS) assay (Hongbo et al., 2005)